Spin-coated ZnO thin films: deposition parameters and crystallinity
Assisted a graduate project on how spin speed and annealing temperature govern crystallite size in sol-gel ZnO films.
- Role
- Undergraduate research assistant
- Supervisor
- Dr. Anucha Wongsri
- Lab
- Thin Film and Surface Science Laboratory, SCME, Mahidol University
- Dates
- Jun – Nov 2025
I supported a graduate student''s study of sol-gel ZnO films on glass substrates, preparing precursor solutions, running the spin coater across a matrix of speeds and annealing temperatures, and collecting the resulting XRD and UV-Vis data.
My contribution was the deposition matrix and the data workup rather than the study design. I learned substrate cleaning discipline the hard way: my first fortnight of films were unusable because of incomplete degreasing.
Key result
Produced and characterised 48 films across a 4×4 speed/temperature matrix; Scherrer analysis showed crystallite size rising from 18 nm to 31 nm between 400 °C and 600 °C annealing.
Methods and techniques
- Sol-gel synthesis
- Spin coating
- XRD
- UV-Vis spectroscopy
- Profilometry
- Annealing