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Spin-coated ZnO thin films: deposition parameters and crystallinity

Assisted a graduate project on how spin speed and annealing temperature govern crystallite size in sol-gel ZnO films.

Role
Undergraduate research assistant
Supervisor
Dr. Anucha Wongsri
Lab
Thin Film and Surface Science Laboratory, SCME, Mahidol University
Dates
Jun – Nov 2025

I supported a graduate student''s study of sol-gel ZnO films on glass substrates, preparing precursor solutions, running the spin coater across a matrix of speeds and annealing temperatures, and collecting the resulting XRD and UV-Vis data.

My contribution was the deposition matrix and the data workup rather than the study design. I learned substrate cleaning discipline the hard way: my first fortnight of films were unusable because of incomplete degreasing.

Key result

Produced and characterised 48 films across a 4×4 speed/temperature matrix; Scherrer analysis showed crystallite size rising from 18 nm to 31 nm between 400 °C and 600 °C annealing.

Methods and techniques

  • Sol-gel synthesis
  • Spin coating
  • XRD
  • UV-Vis spectroscopy
  • Profilometry
  • Annealing